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. 2022 Jun 28;7(27):23736–23743. doi: 10.1021/acsomega.2c02380

Table 1. 1H (850 MHz) and 13C NMR (212.5 MHz) Data for Compound 1 in CD3OD (δ ppm)a.

position δH (J in Hz) δCb
2   176.2 C
3 4.55 s 70.1 CH
4   75.5 C
4.41 d (10.0) 72.3 CH2
4.26 d (10.0)  
6a 4.39 d (11.5) 64.6 CH2
6b 4.43 d (11.5)  
1′   120.4 C
2′ 7.59 d (2.0) 112.3 CH
3′   147.4 C
4′   151.8 C
5′ 6.86 d (8.0) 114.6 CH
6′ 7.61 dd (8.0, 2.0) 123.9 CH
7′   166.2 C
3′-OCH3 3.91 s 54.9 CH3
a

Coupling constants (Hz) are given in parentheses.

b

13C NMR data were assigned based on HSQC and HMBC experiments.