Table 2.
NMR and refinement statistics.
|
NMR distance and dihedral restraints |
Neh1‐ΔLZIP (BMRB 34617, PDB 7O7B) |
|---|---|
|
Distance restraints |
|
|
Total NOE |
337 |
|
Intraresidual (i=j) |
182 |
|
Sequential (i–j=1) |
77 |
|
Medium range (1<i–j<5) |
34 |
|
Long range (i–j≥5) |
44 |
|
Total Dihedral restraints |
92 |
|---|---|
|
ϕ |
46 |
|
ψ |
46 |
|
Structure Statistics |
|
|---|---|
|
Violations (mean±SD) |
|
|
Distance restraints (Å) |
0.09±0.01 |
|
Dihedral restraints (°) |
0.97±0.12 |
|
Deviation from idealized geometry |
|
|---|---|
|
Bond length (Å) |
0.0034±0.0001 |
|
Bond angles (°) |
0.50±0.02 |
|
Ramachandran statistics |
|
|---|---|
|
Residues in allowed regions |
96.1 % |
|
Residues in disallowed regions |
3.9 % |
|
Average pairwise rmsd (Å) |
|
|---|---|
|
Heavy atoms (2° structure) |
1.07±0.08 |
|
Backbone atoms (2° structure) |
0.42±0.07 |