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. 2021 Oct 29;2021(46):4762–4775. doi: 10.1002/ejic.202100722

Figure 4.

Figure 4

Aromatic region of the 1H NMR spectra of 3 at different temperatures (500 MHz, d6 ‐DMSO). At room temperature, three species are observable. Above 70 °C, the broad resonances of 3‐A have disappeared and only 3‐M and 3‐D remain. At the highest temperature, 3‐M dominates the spectrum. As the 25 °C spectrum after the temperature elevation (top spectrum) is equal to the initial 25 °C spectrum before the VT NMR experiment (bottom spectrum), the observed processes are reversible.