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(a) Synthesis of [Rh(Cy2PCH2CH2PCy2)(η2,η2‐norbornane)][BArF 4]; (b) photochemical synthesis of manganese propane and butane complexes; (c) synthesis of rhodium methane complex by protonation; (d) experimental structure of cation [Rh(Cy2PCH2CH2PCy2)(η2,η1‐2‐methylbutane)]+ showing coordination at rhodium by the alkane and calculated structure of CpRe(CO)2(η2‐CH4) at CCSD(T)/def2‐QZVPP level. [48]
