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Deprotection of indolyl alanine 11 b by heating in water.
|
Entry |
T [°C] |
t [h] |
Yield [%] |
ee [%] |
|---|---|---|---|---|
|
1 |
110 |
48 |
83 |
84 |
|
2 |
110 |
24 |
88 |
90 |
|
3 |
110 |
4 |
60 |
92 |
|
4 |
100 |
4 |
18 |
94 |
