Skip to main content
. 2021 Dec 2;23(1):e202100467. doi: 10.1002/cbic.202100467

Scheme 5.

Scheme 5

A) Synthetic scheme for preparation of BC‐cSal (22 a) and BC‐cSal*Na (22 b). Reagents and conditions: a) NaBH4, CH2Cl2, EtOH, AcOH, 0 °C, 3 h, 73 %; b) CBr4, PPh3, CH2Cl2, 0 °CRT, 6 h, 96 %; c) ethyl salicylate, K2CO3, acetone, RT, 2 d, 92 %; d) KOH (0.2 m), MeOH, 60 °C, 4 h, 92 %; e) NaOH (0.2 m), MeOH, RT, 5 min, quant. B) Absorption spectrum of compound 22 a.