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. 2021 Dec 16;28(9):e202103132. doi: 10.1002/chem.202103132

Table 3.

Zinc‐ NPs syntheses in continuous flow.

Oxide

Reactants

Methodology

Year

T

Shape

Size[a] [nm]

Size distribution [σd/d]

Ref.

ZnO

ZnCl2+NH4(CO2NH2)

FIS

1999

RT

rods

10–15[b]

[44]

ZnO

Zn(AcO)2+NaOH

microreactor chip

2014

60 °C

spherical

3–5

[45]

ZnO

Zn(AcO)2+TMAOH (w/an organic acid)

convective tangential micromixer+coil reactor

2014

20–80 °C

3.7[c]

0.11[c]

[51]

ZnO

Zn(NO3)2+NaOH (microemulsions)

micromixer+coil reactor

2014

40–70 °C

10–20[d]

[49]

ZnO

Zn(NO3)2+NaOH

microreactor chips

2017

60 °C

spheres

10 nm

[46]

spindles

300–600 nm

ZnO

Zn(AcO)2+NaOH

droplet‐based mircroreactor

2017

spherical

49.6

0.16

[50]

ZnO

Zn(NO3)2+NaOH

spiral microreactor

2019

RT

spheres

583

0.21

[47]

cubes

153

0.24

[a] Calculated by TEM/SEM analysis. [b] Diameter. [c] At 20 °C. [d] The NPs size depended on the employed conditions (flow rate, T, zinc concentration) fairly monodispersed NPs were obtained in single runs.