TABLE 1.
1H NMR and13C NMR data of compound 1 in MeOH (700 MHz).
NO. | H | C |
---|---|---|
1 | — | 126.4 |
2 | 7.53, d,J = 8.7 Hz | 130.6 |
3 | 6.76, d,J = 8.7 Hz | 115.6 |
4 | — | 163.0 |
5 | 6.76, d,J = 8.7 Hz | 115.6 |
6 | 7.53, d,J = 8.7 Hz | 130.6 |
1′ | — | 114.2 |
2′ | — | 163.9 |
3′ | — | 113.1 |
4′ | — | 160.4 |
5′ | 6.54, d,J = 8.9 Hz | 102.0 |
6′ | 7.94, d,J = 8.9 Hz | 130.2 |
α | 7.72, d,J = 15.3 Hz | 116.9 |
β | 7.55, d,J = 15.3 Hz | 144.6 |
1″ | 2.76 m,2.85 m | 24.0 |
2″ | 4.51 t, J = 7.3 Hz | 87.8 |
3″ | — | 144.7 |
4″ | 4.57 m,4.67 t, J = 1.8 Hz | 112.1 |
4′-OCH3 | 3.80 s | 54.9 |
3″-CH3 | 1.71 s | 15.7 |
C=O | — | 192.8 |