Table 2. Data Collection and Refinement Statistics of the 14-3-3εΔC:FOXO3apS253 Complex Structurea.
| Parameters | 14-3-3ε:FOXO3a |
|---|---|
| Wavelength (Å) | 0.97947 |
| Space group | C2221 |
| Unit cell parameters | |
| a, b, c (Å) | 77.88, 81.04, 83.28 |
| α, β, γ (deg) | 90 90 90 |
| Resolution (Å) | 36.44–1.85 (1.95–1.85) |
| Rmerge (%) | 12.0 (74.3) |
| Mean [⟨I⟩/σ(⟨I⟩)] | 9.8 (2.6) |
| CC (1/2) (%) | 99.4 (77.3) |
| Total no. of reflections | 139,586 (18,464) |
| Unique reflections | 22,570 (3185) |
| Completeness (%) | 99.4 (98.1) |
| Multiplicity | 6.2 (5.8) |
| Molecules in asymmetric unit | 1 |
| Solvent content (%) | 47.61 |
| Refinement statistics | |
| Resolution (Å) | 36.44–1.85 (1.95–1.85) |
| Rwork (%) | 16.65 (25.7) |
| Rfree (%) | 18.88 (26.4) |
| Mean B-value (Å2) | 24.09 |
| Ramachandran favored (%) | 95.5 |
| Ramachandran allowed (%) | 4.5 |
| Ramachandran outlier (%) | 0 |
| rms deviations | |
| Bond length (Å) | 0.013 |
| Bond angle (deg) | 1.750 |
a
Values in parentheses correspond to the highest resolution shell.