Table 3.
Control experiments of synthesis of benzamide from 2-phenylethanol
| Entry | Variation from standard conditions | Conversion of 1 (%) | Yields of 2 (%) |
|---|---|---|---|
| 1 | none | 100 | 93 |
| 2 | loading of MnOx: 30 mg | 100 | 90 |
| 3 | loading of MnOx: 50 mg | 100 | 85 |
| 4 | thickness of autoclave: 15 mm | 100 | 90 |
| 5 | thickness of autoclave: 10 mm | 100 | 90 |
| 6 | reaction temperature: 130°C | 88 | 51 |