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. 2022 Jul 18;3(3):101564. doi: 10.1016/j.xpro.2022.101564

Table 3.

Control experiments of synthesis of benzamide from 2-phenylethanol

Entry Variation from standard conditions Conversion of 1 (%) Yields of 2 (%)
1 none 100 93
2 loading of MnOx: 30 mg 100 90
3 loading of MnOx: 50 mg 100 85
4 thickness of autoclave: 15 mm 100 90
5 thickness of autoclave: 10 mm 100 90
6 reaction temperature: 130°C 88 51