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Reaction scope for aryl radical generation.
aStandard conditions used: 5.9 nm CdS QDs (0.002 mol%), TAEA (1.5 equiv), DMPU (1 mL), blue LEDs, rt. Isolated yields unless otherwise specified. b4 mmol scale, conducted in a Penn PhD M2 photoreactor (See SI for details). cDIPEA (4 equiv) used instead of TAEA. dNaCHO2 (3 equiv) used instead of TAEA. eNMR yield vs CH2Br2.
