Table 2.
Entry | Photocatalyst | Yield of 2aa | TON (per cat.) | mg pdt. / mg cat. |
---|---|---|---|---|
1 | 5.9 nm CdS QDs (0.002 mol%) | 95% | 47500 | 33 |
2 | 4-CzIPN (10 mol%) | 24% | 2.4 | 0.66 |
3 | 4-DPAIPN (10 mol%) | 96% | 9.6 | 2.7 |
4 | [Ir(dFCF3ppy)2(dtbbpy)]PF6 (2 mol%) | 54% | 27 | 5.3 |
5 | PDI (10 mol%) | 16% | 1.6 | 0.59 |
Corrected GC-FID yields vs n-dodecane as internal standard. For experimental details, see Supporting Information Figure S2.