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. 2019 Jun 26;27(4):906–914. doi: 10.1016/j.jfda.2019.06.001

Table 3.

Validation results of recovery and matrix effects.

Compound Nominal conc. (ng/mL) Recovery (%) Matrix effect%
Amlodipine 15 102.69 2.32
150 100.75 −8.53
1500 92.08 3.11
Atenolol 25 95.96 5.81
250 103.29 −3.46
2500 104.72 4.54
Atorvastatin 1 106.50 1.68
10 103.46 3.39
100 99.42 2.66
Digoxin 10 98.08 0.78
100 97.61 5.71
1000 91.04 0.58
Enalapril 0.5 106.54 0.41
5 90.07 −0.85
50 96.13 3.20
Fenofibrate 15 103.49 1.16
150 103.03 −4.35
1500 100.54 −4.33
Furosemide 100 85.63 6.47
1000 98.92 2.31
10000 92.01 −2.62
Losartan 10 104.38 2.75
100 97.56 −1.43
1000 92.45 7.13
Nifedipine 25 88.91 2.83
250 94.19 3.90
2500 87.99 1.26
Propranolol 1 93.68 3.16
10 91.56 −7.05
100 92.99 −3.21
Simvastatin 25 102.17 3.18
250 102.36 −0.84
2500 90.44 1.61
Valsartan 50 87.20 2.04
500 91.54 −1.99
5000 85.46 4.23