Table 3.
Compound | Nominal conc. (ng/mL) | Recovery (%) | Matrix effect% |
---|---|---|---|
Amlodipine | 15 | 102.69 | 2.32 |
150 | 100.75 | −8.53 | |
1500 | 92.08 | 3.11 | |
Atenolol | 25 | 95.96 | 5.81 |
250 | 103.29 | −3.46 | |
2500 | 104.72 | 4.54 | |
Atorvastatin | 1 | 106.50 | 1.68 |
10 | 103.46 | 3.39 | |
100 | 99.42 | 2.66 | |
Digoxin | 10 | 98.08 | 0.78 |
100 | 97.61 | 5.71 | |
1000 | 91.04 | 0.58 | |
Enalapril | 0.5 | 106.54 | 0.41 |
5 | 90.07 | −0.85 | |
50 | 96.13 | 3.20 | |
Fenofibrate | 15 | 103.49 | 1.16 |
150 | 103.03 | −4.35 | |
1500 | 100.54 | −4.33 | |
Furosemide | 100 | 85.63 | 6.47 |
1000 | 98.92 | 2.31 | |
10000 | 92.01 | −2.62 | |
Losartan | 10 | 104.38 | 2.75 |
100 | 97.56 | −1.43 | |
1000 | 92.45 | 7.13 | |
Nifedipine | 25 | 88.91 | 2.83 |
250 | 94.19 | 3.90 | |
2500 | 87.99 | 1.26 | |
Propranolol | 1 | 93.68 | 3.16 |
10 | 91.56 | −7.05 | |
100 | 92.99 | −3.21 | |
Simvastatin | 25 | 102.17 | 3.18 |
250 | 102.36 | −0.84 | |
2500 | 90.44 | 1.61 | |
Valsartan | 50 | 87.20 | 2.04 |
500 | 91.54 | −1.99 | |
5000 | 85.46 | 4.23 |