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. 2019 Mar 12;27(3):703–716. doi: 10.1016/j.jfda.2019.02.004

Table 1.

MRM parameter and retention times for 21 coccidiostats.

Analyte RTa (min) DPb (V) Precursor ion (m/z) For quantification For conformation


Product ion (m/z) CEc (eV) CXPd (V) Product ion (m/z) CE (eV) CXP (V)
Buqinolate 15.8 50 361.8 204.0 50 20 260.2 40 20
Clopidol 7.7 60 192.0 101.0 38 15 103.0 39 10
Closantel 17.6 −40 660.9 127.1 −46 −10 315.0 −46 −20
Decoquinate 17.6 50 418.2 372.4 35 20 204.2 58 15
Diaveridine 7.3 50 261.0 245.2 37 15 123.0 37 20
Dicalzuril 15.1 −40 407.0 335.9 −26 −20 334.1 −26 −20
Dimetridazole 6.3 50 142.0 96.0 24 15 81.0 39 10
Diminazene aceturate 7.4 30 282.2 119.2 26 15 135.2 13 15
Ethopabate 11.5 30 238.0 135.9 39 15 206.0 16 15
Halofuginone 11.4 50 416.1 100.1 30 15 120.2 30 15
Imidocarb 6.9 60 349.2 145.0 76 20 188.2 46 15
Isometamidium 10.4 60 460.3 313.2 29 20 298.3 31 20
Levamisole 6.8 50 204.8 123.0 40 15 117.2 40 15
Metronidazole 6.2 45 172.1 128.3 45 15 82.1 32 10
Nicarbazin 14.4 −60 301.0 137.2 −20 −15 107.1 −50 −15
Novobiocin 16.1 65 613.1 189.3 65 20 396.3 22 20
Praziquantel 14.3 50 313.1 203.3 50 10 174.2 40 15
Pyrantel pamoate 7.9 50 207.1 150.1 50 15 136.1 42 15
Pyrimethamine 10.6 40 249.0 177.1 40 10 198.2 55 25
Robenidine 14.1 30 334.2 110.9 61 25 138.1 35 20
Zoalene 9.0 −40 224.1 181.1 −15 −20 151.3 −22 −20
a

RT: Retention time (min).

b

DP: Declustering potential.

c

CE: Collision energy.

d

CXP: Collision cell exit potential.