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. 2022 Jul 19;37(1):2017–2035. doi: 10.1080/14756366.2022.2101645

Scheme 2.

Scheme 2.

Reagents and conditions: (g) TBTU, Et3N, DCM, ice-bath; (h) DCM, TFA; TBTU, Et3N, DCM, ice-bath.