Table 6.

Method performance characteristics in neat solvent and cereal matrices.

Analyte	Curve Type	Equation	Concentration Range [µg/kg]	Linearity R2	LOD µg/kg	LOQ µg/kg
AFB1	Solvent	y = 4233.3x − 151.78	1.0–16	0.9966	0.30	1.0
	Wheat	y = 3255.2x − 33.549		0.9985
	Maize	y = 1243.3x − 19.301		0.9993
	Barley	y = 3405.3x − 97.552		0.9995
AFB2	Solvent	y = 3330.9x − 92.654	0.5–10	0.9995	0.15	0.5
	Wheat	y = 2294.8x − 0.6601		0.9998
	Maize	y = 821.52x − 31.61		0.9995
	Barley	y = 2520.2x − 32.659		0.9998
AFG1	Solvent	y = 3933.1x − 31.126	1.0–16	0.9976	0.30	1.0
	Wheat	y = 2902x + 27.304		0.9981
	Maize	y = 976.96x − 14.994		1.0000
	Barley	y = 1502.5x − 145.4		0.9989
AFG2	Solvent	y = 3330.9x − 92.654	0.5–10	0.9995	0.15	0.5
	Wheat	y = 3502.6x − 9.2733		0.9997
	Maize	y = 1075.8 − 21.436		0.9999
	Barley	y = 2394.8x − 0.6601		0.9998
DON	Solvent	y = 14.19x + 40.633	200–4000	0.9999	61	200
	Wheat	y = 8.4400x + 3.6843		0.9992
	Maize	y = 8.7478x + 11.739		0.9997
	Barley	y = 8.3797x − 2.8576		0.9999
FB1	Solvent	y = 198.06x − 3113	150–3000	0.9966	46	150
	Wheat	y = 230.94x − 866.12		0.9991
	Maize	y = 103.05x − 167.52		1.0000
	Barley	y = 237.94x − 866.12		0.9999
FB2	Solvent	y = 761.01x − 16822	150–3000	0.9945	46	150
	Wheat	y = 493.7x − 4122.5		0.9966
	Maize	y = 209.36x − 598.27		0.9999
	Barley	y = 578.72x − 7184.9		0.9985
ZEA	Solvent	y = 91.077x + 3.8326	30–600	0.9997	9	30
	Wheat	y = 70.491x + 72.751		0.9992
	Maize	y = 26.71x + 35.167		0.9993
	Barley	y = 70.654x − 22.304		0.9999
T-2	Solvent	y = 696.5x − 134.59	10–200	0.9996	3	10
	Wheat	y = 757.94x + 36.431		0.9996
	Maize	y = 267.43x − 69.004		1.0000
	Barley	y = 760.5x + 36.722		0.9999
HT-2	Solvent	y = 98.501x − 56.058	10–200	0.9975	3	10
	Wheat	y = 97.296x + 87.819		0.9997
	Maize	y = 39.128x + 12.603		0.9996
	Barley	y = 115.99x + 58.863		0.9999
OTA	Solvent	y = 1049.8x − 52.161	1.0–20	0.9979	0.30	1.0
	Wheat	y = 853.76x − 68.076		0.9992
	Maize	y = 375.68 − 42.071		0.9991
	Barley	y = 889.28x − 14.52		0.9964