Table 1.

Synthesis procedure for the different samples.

Sample Family	Synthesis Route Type	Sample	Thermo-Mechanic Treatment
			Milling (h)	Annealing (°C)
A	Commercially supplied	A1	-	1100, 24 h
		A2	50
		A3	50	400, 1 h
		A4	50	500, 1 h
B	Ceramic	B1		1200, 24 h
		B2	2
		B3	10
		B4	50
C	Mechano-Synthesis	C1	150
		C2	150	300, 1 h
		C3	150	400, 1 h
		C4	150	500, 1 h
		C5	150	600, 1 h