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. 2022 Jul 3;10(7):1346. doi: 10.3390/microorganisms10071346

Table 3.

Glycosyl linkage analysis of cranberry A6 fractions.

Linkage A6 A A6 B A6 C
t-Araf 5.7 5.5 7.7
t-Fucp 0.1 0.3 0.2
t-Arap 0.1 0.3 0.1
t-Xylp 3.3 2.1 3.8
2-Rhap 0.1 0.4 0.7
3-Rhap - 0.2 0.2
t-Manp 0.1 - -
t-Glcp 15.5 26.9 8.1
3-Araf 0.7 1.7 2.5
t-GalfA - - 0.6
t-Galp 2.5 1.6 2.8
t-GalpA 0.2 0.2 0.7
4-Arap or 5-Araf 4.0 8.2 12.0
3’-Apiose - - 0.1
2-Xylp 9.9 4.5 7.0
4-Xylp 1.2 0.9 1.0
3,4-Fucp 0.1 0.1 0.2
3-Glcp 0.3 1.3 -
2,4-Rhap - - 0.5
2-Glcp 0.2 0.4 0.1
2-GlcpA - - 0.1
3-Galp 0.1 - 0.2
4-Manp 0.4 0.2 0.5
3,4-Arap or 3,5-Araf 0.3 1.3 2.5
6-Glcp 5.9 11.7 5.8
4-Galp 0.1 0.1 0.3
4-GalpA 0.4 0.2 1.7
4-Glcp 20.0 17.7 17.4
2,4-Xylp 0.1 0.1 0.1
6-Galp 0.1 0.1 0.3
2,3,4-Arap or 2,3,5-Araf 0.1 0.2 0.9
3,4-Glcp 0.2 0.2 0.3
2,4-Glcp 0.5 0.3 0.4
2,4-GlcpA - - 0.1
3,6-Glcp - - 0.1
4,6-Glcp 27.7 13.2 20.6
3,6-Galp 0.1 - 0.1

Glycosyl-linkage deduced from GC/MS analysis of per-O-methylated alditol acetates. Glycosyl-linkage position (numbers), apiose (Api), arabinose (Ara), fructose (Fru), galactose (Gal), galacturonic acid (GalA), glucose (Glc), glucuronic acid (GlcA), fucose (Fuc), mannose (Man), rhamnose (Rha), xylose (Xyl), furanose (f), pyranose (p), terminal (t) and not detected (-). Relative peak area percentages (%) three cranberry batches (A6 A, A6 B, A6 C) were produced in different years.