Table 3.
Compound | Precisiona | Accuracya | Reproducibility | ||
---|---|---|---|---|---|
|
|
|
|||
Intra-day (RSD, %) | Inter-day (RSD, %) | Intra-day (%) | Inter-day (%) | RSD (%) | |
1 | 2.4–8.9 | 4.2–8.4 | 96.8–111.6 | 96.6–108.7 | 1.3 |
2 | 0.8–5.1 | 4.0–6.3 | 94.7–104.3 | 93.8–100.3 | 3.0 |
3 | 1.4–3.6 | 1.6–9.1 | 96.5–106.6 | 96.3–110.6 | 2.2 |
4 | 0.8–2.3 | 1.7–4.7 | 97.3–102.8 | 97.4–103.5 | 2.2 |
5 | 0.8–4.5 | 2.2–5.7 | 95.0–106.3 | 100.0–106.5 | 3.3 |
6 | 1.2–8.5 | 3.1–8.9 | 101.4–111.0 | 96.3–102.6 | 2.4 |
7 | 1.1–4.0 | 0.8–4.8 | 93.7–103.6 | 99.1–102.2 | 2.6 |
8 | 1.6–2.5 | 1.2–8.2 | 97.5–109.2 | 96.0–102.7 | 2.3 |
9 | 5.1–6.9 | 0.7–9.9 | 90.5–96.6 | 99.0–101.6 | 2.1 |
10 | 4.6–10.9 | 4.9–7.6 | 93.4–107.8 | 100.3–106.5 | 2.4 |
11 | 0.1–5.3 | 0.7–9.1 | 98.8–109.0 | 97.0–105.3 | 2.5 |
12 | 1.7–4.5 | 2.9–11.8 | 99.0–103.5 | 98.7–112.8 | 2.2 |
13 | 1.1–4.6 | 2.4–3.7 | 99.0–103.9 | 101.5–103.1 | 2.1 |
14 | 0.5–5.8 | 2.6–11.3 | 97.4–100.2 | 99.1–110.1 | 2.7 |
15 | 1.7–4.2 | 2.1–6.8 | 96.0–100.4 | 97.0–101.6 | 2.4 |
16 | 1.4–2.0 | 3.2–6.0 | 97.2–101.2 | 100.8–103.9 | 4.7 |
Three different concentration levels (n = 3).