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. 2017 Jul 8;26(2):572–582. doi: 10.1016/j.jfda.2017.06.002

Table 3.

Intra- and inter-day precision, accuracy (n =3) and reproducibility (n =6) of HCAA compounds.

Compound Precisiona Accuracya Reproducibility



Intra-day (RSD, %) Inter-day (RSD, %) Intra-day (%) Inter-day (%) RSD (%)
1 2.4–8.9 4.2–8.4 96.8–111.6 96.6–108.7 1.3
2 0.8–5.1 4.0–6.3 94.7–104.3 93.8–100.3 3.0
3 1.4–3.6 1.6–9.1 96.5–106.6 96.3–110.6 2.2
4 0.8–2.3 1.7–4.7 97.3–102.8 97.4–103.5 2.2
5 0.8–4.5 2.2–5.7 95.0–106.3 100.0–106.5 3.3
6 1.2–8.5 3.1–8.9 101.4–111.0 96.3–102.6 2.4
7 1.1–4.0 0.8–4.8 93.7–103.6 99.1–102.2 2.6
8 1.6–2.5 1.2–8.2 97.5–109.2 96.0–102.7 2.3
9 5.1–6.9 0.7–9.9 90.5–96.6 99.0–101.6 2.1
10 4.6–10.9 4.9–7.6 93.4–107.8 100.3–106.5 2.4
11 0.1–5.3 0.7–9.1 98.8–109.0 97.0–105.3 2.5
12 1.7–4.5 2.9–11.8 99.0–103.5 98.7–112.8 2.2
13 1.1–4.6 2.4–3.7 99.0–103.9 101.5–103.1 2.1
14 0.5–5.8 2.6–11.3 97.4–100.2 99.1–110.1 2.7
15 1.7–4.2 2.1–6.8 96.0–100.4 97.0–101.6 2.4
16 1.4–2.0 3.2–6.0 97.2–101.2 100.8–103.9 4.7
a

Three different concentration levels (n = 3).