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. 2022 Jul 11;12(7):633. doi: 10.3390/metabo12070633

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© 2022 by the authors.

Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).

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Extracted ion chromatograms of 26 unconjugated (a), 8 glycine-conjugated and 9 taurine-conjugated BAs (b), 5 taurine-sulfated, 5 glycine-sulfated, and 5 sulfated BAs (c), and 15 deuterium (D)-labeled BAs as Internal Standards (d). (1) UCA (2) 7,12-diketoLCA (3) DHCA (4) ω-MCA (5) α-MCA (6) 7-DHCA (7) β-MCA (8) γ-MCA (9) MDCA (10) 3-DHCA (11) alloCA (12) CA (13) UDCA (14) HDCA (15) 7-ketoLCA (16) 6,7-diketoLCA (17) norDCA (18) apoCA (19)12-ketoLCA (20) CDCA (21) DCA (22) isoalloLCA (23) isoDCA (24) isoLCA (25) LCA (26) 3-ketoLCA (27) T-α-MCA (28) T-β-MCA (29) GDHCA (30) THCA (31) TUDCA (32) THDCA (33) GHCA (34) TCA (35) GHDCA (36) GCA (37) GUDCA (38) TCDCA (39) TDCA (40) GDCA (41) GCDCA (42) TLCA (43) GLCA (44) TUDCA-3S (45) TCA-3S (46) GUDCA-3S (47) GCA-3S (48) TCDCA-3S (49) TDCA-3S (50) GCDCA-3S (51) GDCA-3S (52) TLCA-3S (53) UDCA-3S (54) CA-3S (55) GLCA-3S (56) CDCA-3S (57) DCA-3S (58) LCA-3S (IS1) TUDCA-3S-d4 (IS2) TCA-d4 (IS3) GDCA-3S-d4 (IS4) GUDCA-d4 (IS5) GCA-d4 (IS6) TCDCA-d5 (IS7) CDCA-3S-d4 (IS8) GDCA-d4 (IS9) GCDCA-d4 (IS10) CA-d4 (IS11) UDCA-d4 (IS12) GLCA-d4 (IS13) CDCA-d4 (IS14) DCA-d4 (IS15).