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. 2022 Jul 8;16(7):10545–10553. doi: 10.1021/acsnano.2c01948

Figure 1.

Figure 1

XPEEM setup and exfoliated Fe5GeTe2 flake. (a) Experimental XPEEM setup and layered Fe5GeTe2 crystal structure on an Au underlayer. The sample was capped with an amorphous Se (a-Se) layer. (b) Optical micrograph showing exfoliated flake with trilayer (3L, marked by a dotted line), four-layer (4L), and bulk-like (nL) regions. The thicknesses have been cross-calibrated with atomic force microscopy (Figure S2) and via the intensity of the L3 absorption peak. (c) Spatial XAS scan of an ultrathin mono- and bilayer area of the sample. The spatial integration of the XAS spectra over the three colored areas (see XPEEM image in inset) reveals metallic Fe L3 and L2 edges, indicating the absence of oxidation (see Figure S3 for the spectrum of oxidized Fe5GeTe2).