TABLE 2.
Instrumental conditions of PerkinElmer Optima 4300DV ICP-OES.
ICP source operation parameters | |
---|---|
RF power | 1300 W |
Plasma gas flow | Ar 15 L min−1 |
Auxiliary gas flow | Ar 0.2 L min−1 |
Nebulizer gas flow | Ar 0.7 L min−1 |
Nebulizer | Borosilicate glass conical nebulizer |
Spray chamber | Borosilicate glass cyclonic spray chamber |
Sample uptake | 1 ml min−1 |
Spectrometer operating parameters | |
Viewing direction | Axial |
Signal measurement mode | Peak area (3 point) |
Background correction | Manually selected, 2 point interpolations |
Measurement time | Auto |
Measurement replications | Ten times |
Measured emission line | La: 407.735 nm, Co: 238.892 nm |