TABLE 4.
| Run no. | Sample mass, g | Recovered La2O3, g | Unprecipitated La, μg | La in precipitate, % | Unprecipitated La, % | Purity of original La2O3 c , % |
|---|---|---|---|---|---|---|
| 1 | 0.94130 | 0.94062 | 386 ± 4.1 | 99.928 | 0.048 | 99.976 ± 0.003 |
| 2 | 0.95886 | 0.95874 | 525 ± 4.8 | 99.988 | 0.064 | 100.052 ± 0.009 |
| 3 | 0.77350 | 0.77274 | 474 ± 4.2 | 99.901 | 0.072 | 99.973 ± 0.005 |
| 4 | 0.87258 | 0.87149 | 467 ± 4.2 | 99.875 | 0.063 | 99.938 ± 0.003 |
| 5 | 0.99128 | 0.99056 | 370 ± 3.6 | 99.928 | 0.044 | 99.972 ± 0.005 |
| 6 | 0.87286 | 0.87206 | 515 ± 4.0 | 99.908 | 0.069 | 99.977 ± 0.006 |
| 7 | 0.86632 | 0.86570 | 492 ± 4.6 | 99.928 | 0.067 | 99.995 ± 0.005 |
| 8 | 0.88910 | 0.88874 | 420 ± 3.4 | 99.959 | 0.055 | 100.014 ± 0.011 |
| 9 | 0.85972 | 0.85850 | 553 ± 3.5 | 99.859 | 0.075 | 99.934 ± 0.006 |
| 10 | 0.98191 | 0.98119 | 532 ± 3.8 | 99.926 | 0.064 | 99.990 ± 0.005 |
| Mean | 99.982 ± 0.012 | |||||
Calculated based on the weighing form as La2O3.
Each value following "±" indicates the combined standard uncertainty (k = 1).
The purity value of original La2O3 was corrected by the mass fraction of impurities.