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. 2022 Jul 15;10:888636. doi: 10.3389/fchem.2022.888636

TABLE 4.

Analytical results for purity of the original La2O3 sample by the oxide weighing method a , b .

Run no. Sample mass, g Recovered La2O3, g Unprecipitated La, μg La in precipitate, % Unprecipitated La, % Purity of original La2O3 c , %
1 0.94130 0.94062 386 ± 4.1 99.928 0.048 99.976 ± 0.003
2 0.95886 0.95874 525 ± 4.8 99.988 0.064 100.052 ± 0.009
3 0.77350 0.77274 474 ± 4.2 99.901 0.072 99.973 ± 0.005
4 0.87258 0.87149 467 ± 4.2 99.875 0.063 99.938 ± 0.003
5 0.99128 0.99056 370 ± 3.6 99.928 0.044 99.972 ± 0.005
6 0.87286 0.87206 515 ± 4.0 99.908 0.069 99.977 ± 0.006
7 0.86632 0.86570 492 ± 4.6 99.928 0.067 99.995 ± 0.005
8 0.88910 0.88874 420 ± 3.4 99.959 0.055 100.014 ± 0.011
9 0.85972 0.85850 553 ± 3.5 99.859 0.075 99.934 ± 0.006
10 0.98191 0.98119 532 ± 3.8 99.926 0.064 99.990 ± 0.005
Mean 99.982 ± 0.012
a

Calculated based on the weighing form as La2O3.

b

Each value following "±" indicates the combined standard uncertainty (k = 1).

c

The purity value of original La2O3 was corrected by the mass fraction of impurities.