TABLE 6.
Uncertainties about the reproducibility of the gravimetric analysis and the stoichiometry of weighing forms.
Run no. | Purity of original La2O3 by oxide form, % | Purity of original La2O3 by sulfate form, % | Mean of the purity values a , % | Absolute difference of the purity values b , % | , % |
---|---|---|---|---|---|
1 | 99.976 ± 0.003 | 99.947 ± 0.008 | 99.961 | 0.030 | 0.017 |
2 | 100.052 ±0.009 | 99.978 ± 0.006 | 100.015 | 0.074 | 0.043 |
3 | 99.973 ± 0.005 | 100.049 ± 0.007 | 100.011 | 0.075 | 0.043 |
4 | 99.938 ± 0.003 | 99.948 ± 0.008 | 99.943 | 0.010 | 0.0058 |
5 | 99.972 ± 0.005 | 99.963 ± 0.006 | 99.967 | 0.0085 | 0.0049 |
6 | 99.977 ± 0.006 | 99.965 ± 0.013 | 99.971 | 0.012 | 0.0069 |
7 | 99.995 ± 0.005 | 99.942 ± 0.007 | 99.968 | 0.053 | 0.030 |
8 | 100.014 ± 0.011 | 99.974 ± 0.006 | 99.994 | 0.040 | 0.023 |
9 | 99.934 ±0.006 | 99.962 ± 0.006 | 99.948 | 0.029 | 0.016 |
10 | 99.990 ± 0.005 | 100.001 ± 0.008 | 99.996 | 0.012 | 0.0069 |
Mean | 99.977 | Root mean square | 0.024 c | ||
RSD | 0.025 | ||||
0.0080 d |
Mean of the purity values obtained in the two weighing forms.
Absolute difference in purity values obtained from two weighing forms.
The root mean square was used as uncertainty for the stoichiometry of weighing forms.
The was used as uncertainty of the reproducibility of the gravimetric analysis.