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. 2022 Jul 15;10:888636. doi: 10.3389/fchem.2022.888636

TABLE 6.

Uncertainties about the reproducibility of the gravimetric analysis and the stoichiometry of weighing forms.

Run no. Purity of original La2O3 by oxide form, % Purity of original La2O3 by sulfate form, % Mean of the purity values a , % Absolute difference of the purity values b , % |Dif.|/3 , %
1 99.976 ± 0.003 99.947 ± 0.008 99.961 0.030 0.017
2 100.052 ±0.009 99.978 ± 0.006 100.015 0.074 0.043
3 99.973 ± 0.005 100.049 ± 0.007 100.011 0.075 0.043
4 99.938 ± 0.003 99.948 ± 0.008 99.943 0.010 0.0058
5 99.972 ± 0.005 99.963 ± 0.006 99.967 0.0085 0.0049
6 99.977 ± 0.006 99.965 ± 0.013 99.971 0.012 0.0069
7 99.995 ± 0.005 99.942 ± 0.007 99.968 0.053 0.030
8 100.014 ± 0.011 99.974 ± 0.006 99.994 0.040 0.023
9 99.934 ±0.006 99.962 ± 0.006 99.948 0.029 0.016
10 99.990 ± 0.005 100.001 ± 0.008 99.996 0.012 0.0069
Mean 99.977 Root mean square 0.024 c
RSD 0.025
RSD/n 0.0080 d
a

Mean of the purity values obtained in the two weighing forms.

b

Absolute difference in purity values obtained from two weighing forms.

c

The root mean square was used as uncertainty for the stoichiometry of weighing forms.

d

The RSD/n was used as uncertainty of the reproducibility of the gravimetric analysis.