Table 1.
Randomized central composite RSM design matrix with un-coded values of the factors
| Run | A: Pressure | B: Time | Consistency coefficient (K) | Flow Behavior Index (n) |
Yield stress | Foaming capacity | Foaming stability | Emulsion capacity | Emulsion stability | Crystallinity 1048/1022 | Particle size | Lightness (L*) |
|---|---|---|---|---|---|---|---|---|---|---|---|---|
| MPa | min | Pa.s | Pa (E-07) | % | min | mL | mL | Ratio (× 10−1) | µm | |||
| 1 | 401 | 18 | 1.08 ± 0.2 | 0.51 ± 0.1 | 8.9 ± 0.0 | 68.3 ± 3.1 | 50.5 ± 5.0 | 5.0 ± 0.0 | 4.3 ± 0.2 | 6.9 ± 0.0 | 139 ± 13.4 | 33.4 ± 0.1 |
| 2 | 542 | 26 | 0.90 ± 0.0 | 0.60 ± 0.0 | 2.2 ± 0.0 | 82.5 ± 2.0 | 14.5 ± 1.5 | 5.2 ± 0.2 | 4.8 ± 0.6 | 7.7 ± 0.1 | 90 ± 5.0 | 28.9 ± 0.0 |
| 3 | 401 | 30 | 1.35 ± 0.7 | 0.45 ± 0.1 | 1.9 ± 0.0 | 75.8 ± 4.2 | 48.0 ± 5.0 | 4.8 ± 0.2 | 4.5 ± 0.4 | 7.7 ± 0.1 | 187 ± 21.6 | 31.8 ± 0.0 |
| 4 | 200 | 18 | 0.43 ± 0.1 | 0.65 ± 0.0 | 2.5 ± 0.0 | 69.2 ± 2.4 | 46.0 ± 1.6 | 5.7 ± 0.5 | 5.3 ± 0.6 | 8.0 ± 0.1 | 224 ± 27.0 | 33.3 ± 0.1 |
| 5 | 401 | 18 | 1.08 ± 0.2 | 0.51 ± 0.1 | 8.9 ± 0.0 | 68.3 ± 3.1 | 50.5 ± 5.0 | 5.0 ± 0.0 | 4.3 ± 0.2 | 6.9 ± 0.0 | 139 ± 13.4 | 33.4 ± 0.1 |
| 6 | 259 | 26 | 0.25 ± 0.1 | 0.65 ± 0.0 | 2.8 ± 0.0 | 80.8 ± 5.0 | 24.7 ± 1.7 | 5.2 ± 0.5 | 4.7 ± 0.5 | 8.0 ± 0.1 | 190 ± 4.0 | 29.9 ± 0.0 |
| 7 | 542 | 9 | 0.30 ± 0.0 | 0.71 ± 0.0 | 8.7 ± 0.0 | 72.5 ± 2.5 | 61.5 ± 9.5 | 5.5 ± 0.7 | 5.3 ± 0.5 | 7.8 ± 0.3 | 320 ± 2.1 | 40.4 ± 0.2 |
| 8 | 259 | 9 | 0.12 ± 0.0 | 0.70 ± 0.0 | 1.1 ± 0.0 | 78.3 ± 5.0 | 67.0 ± 2.0 | 5.0 ± 0.4 | 4.3 ± 0.5 | 7.8 ± 0.1 | 143 ± 6.6 | 49.4 ± 0.6 |
| 9 | 401 | 5 | 0.25 ± 0.1 | 0.66 ± 0.0 | 1.2 ± 0.0 | 72.5 ± 2.0 | 39.5 ± 2.5 | 5.2 ± 0.2 | 4.7 ± 0.2 | 7.3 ± 0.1 | 150 ± 14.8 | 49.6 ± 0.2 |
| 10 | 401 | 18 | 1.08 ± 0.2 | 0.51 ± 0.1 | 8.9 ± 0.0 | 68.3 ± 3.1 | 50.5 ± 5.0 | 5.0 ± 0.0 | 4.3 ± 0.2 | 6.9 ± 0.0 | 139 ± 13.4 | 33.4 ± 0.1 |
| 11 | 601 | 18 | 0.45 ± 0.1 | 0.64 ± 0.0 | 1.9 ± 0.0 | 78.8 ± 3.8 | 53.5 ± 1.5 | 5.7 ± 0.2 | 5.5 ± 0.4 | 7.7 ± 0.3 | 120 ± 2.2 | 27.0 ± 0.0 |
| Control | – | – | 0.65 ± 0.1 | 0.51 ± 0.1 | 2.9 ± 0.0 | 79.2 ± 3.1 | 50.5 ± 1.5 | 4.8 ± 0.2 | 4.8 ± 0.7 | 9.3 ± 0.0 | 24.1 ± 3.5 | 27.5 ± 0.1 |