Official websites use .gov
A
.gov website belongs to an official
government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you've safely
connected to the .gov website. Share sensitive
information only on official, secure websites.
| Parameter | Descriptions |
|---|---|
| Column | QP2010SE, Shimadzu |
| PEG-20M | |
| Length: 30 m | |
| Internal diameter: 0.32 mm | |
| Film thickness: 1 μm | |
| Injector temperature | 220 °C |
| Detector temperature (EI 250) | 210 °C |
| Carrier gas | Helium, flow rate = 1.2 mL min−1 |
| Injection | V = 1 μL |
| Split ratio | Flow rate = 40 : 1 |
| Temperature program | Initial temperature = 100 °C |
| Rate of progression = 10 °C min−1 | |
| Final temperature = 210 °C, 20 min |
