Table 1. Structure and Geometric Parameters of TDO NPs by XRD Analysis.

tem. (°C)	2θ	fwhm value	plane	d-spacing (Å)	cos(θ)	crystalline size (nm)
300	25.69	1.29	(101)	3.48	0.97497	6.60
	38.32	1.68	(004)	2.34	0.94460	5.22
	48.41	1.17	(200)	1.87	0.91208	7.77
	55.37	2.38	(211)	1.67	0.88551	3.94
average size						5.88
500	25.66	0.99	(101)	3.85	0.97503	8.60
	38.29	1.42	(004)	2.61	0.94469	6.18
	48.31	1.09	(200)	2.08	0.91244	8.35
	55.38	1.14	(211)	1.83	0.88547	8.22
average size						7.83
800	25.60	0.30	(101)	3.94	0.97514	28.38
	37.99	0.33	(004)	2.65	0.94554	26.60
	48.36	0.35	(200)	2.08	0.91226	26.00
	54.16	0.37	(105)	1.87	0.89037	25.20
	55.41	0.38	(211)	1.82	0.88535	24.66
average size						25.96