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. 2022 Aug 4;12:13433. doi: 10.1038/s41598-022-17527-y

Table 2.

Repeatability and accuracy of the quantitative determination of 14 active pharmaceutical ingredients with the TLCyzer app. The results of all 168 individual measurements are displayed graphically in Fig. 3, and their numerical values are listed in Supplementary Table S2.

API Conc. (%) Mean (%) (n = 4) SD (%) (n = 4) Relative SD [%] (n = 4) Relative SD [%] (n = 12) Recovery mean (n = 4) [%]
Atenolol 70 72.5 0.59 0.81 2.33 103.5
85 85.9 1.59 1.85 101.1
90 91.7 3.97 4.33 101.8
Ceftriaxone 70 70.1 3.99 5.68 3.50 100.2
85 84.1 1.00 1.18 99.8
90 90.4 3.31 3.63 101.3
Cefuroxime axetil 70 72.0 3.09 4.29 3.70 102.9
85 82.3 2.13 2.59 96.8
90 90.5 3.82 4.23 100.5
Chloroquine 70 68.7 0.93 1.36 1.59 98.1
85 85.5 0.95 1.11 100.5
90 91.9 2.11 2.30 102.1
Ciprofloxacin 70 69.8 1.93 2.77 3.34 99.7
85 84.7 3.53 4.17 99.6
90 92.5 2.86 3.09 102.8
Dexamethasone 70 67.5 2.75 4.08 2.92 96.4
85 85.2 2.07 2.43 100.3
90 92.1 2.08 2.26 102.3
Fluconazole 70 70.4 1.68 2.39 2.40 100.6
85 84.3 1.54 1.82 99.1
90 89.1 2.68 3.01 99.0
Furosemide 70 70.3 1.82 2.59 2.28 100.5
85 85.1 2.20 2.58 100.1
90 92.6 1.54 1.66 102.8
Glibenclamide 70 68.5 2.04 2.98 3.17 97.9
85 83.0 4.34 5.23 97.6
90 90.6 1.17 1.29 100.6
Hydrochloro-thiazide 70 70.8 1.27 1.80 1.98 101.2
85 85.5 1.24 1.45 100.6
90 90.9 2.46 2.70 101.0
Metformin 70 72.0 3.45 4.80 3.21 102.8
85 83.7 1.94 2.32 98.5
90 89.1 2.25 2.53 99.0
Metronidazole 70 69.2 2.38 3.44 2.33 98.8
85 85.0 0.66 0.77 100.0
90 90.0 2.50 2.77 100.0
Sulfamethoxazole 70 70.1 3.38 4.82 3.84 100.2
85 87.4 2.91 3.33 102.8
90 93.5 3.17 3.39 103.9
Trimethoprim 70 68.6 1.53 2.22 2.48 98.0
85 84.0 2.86 3.41 98.8
90 88.2 1.61 1.82 97.9
Mean 2.79 100.3