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. 2022 Jul 26;10:975267. doi: 10.3389/fchem.2022.975267

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Copyright © 2022 Wang, Luo, Wang, Han, Miu, Luo, Zhang and Kuang.

This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms.

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Synthetic route of α-substituted indole-3-acetic acids. Reagents and conditions: a) DCC, DMAP, MeOH, dry CH₂Cl₂, r.t.; b) TEBAC, methyl chloroformate, DCM, 30% NaOH (aq.), ice bath; c) R-Br, LDA, HMPA, THF, −78°C–0°C; d) 30% NaOH (aq.): CH₃OH = 1:2 (v/v), 70°C, 4 h, 2 M HCl.