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(A) Temperature determination for isothermal experiments from the first heating run of polymer P5 (intra) in the nanoparticle conformation. A temperature ramp of 10 K min–1 was used. (B) Isothermal DSC traces between 70 and 85 °C (dotted lines) with corresponding degrees of cure (α) (solid lines). Arrhenius analysis of (C) polymers P4–P6 (intra) and (D) polymers P7–P9 (intra). (E) Activation energy for nanoparticle relaxation shown as a function of grafting density.
