Table 2.
Crystallographic data collection and structure refinement.
| SSL10 | |
|---|---|
| PDB code | 6LWTa |
| Data collection | |
| Space group | P21 21 21 |
| Cell dimensions | |
| a, b, c (Å) | 41.24, 71.21, 140.66 |
| α, β, γ (°) | 90, 90, 90 |
| Resolution (Å) | 50.0–1.90 (1.93–1.90)b |
| Wavelength (Å) | 0.9778 |
| Rsym or Rmerge (%) | 9.0 (29.4) |
| Overall I/σ(I) | 16.2 (7.0) |
| Completeness (%) | 100.0 (100.0) |
| Redundancy | 6.4 (6.6) |
| Refinement | |
| Resolution (Å) | 39.58–1.90 |
| No. reflections | 31,821 |
| Rwork/Rfree (%) | 20.94/24.62 |
| No. atoms | |
| Protein/Water | 3127/57 |
| Average B-factors (Å2) | |
| Protein/Water | 30.858/27.255 |
| R.m.s deviations | |
| Bond lengths (Å) | 0.0088 |
| Bond angles (°) | 1.3524 |
| Ramachandran plotc | |
| Most favored regions (%) | 96.23 |
| Allowed regions (%) | 3.77 |
| Generously allowed regions (%) | 0 |
aOne single crystal of SSL10 was used for the structure determination.
bThe values in parentheses refer to the highest resolution shell.
cStatistics for the Ramachandran plot from an analysis using MolProbity.