Figure 6.

Product distribution using enantiopure mono D-labeled substrates S-9_HD and R-9_HD.^{41, 74} The two pairs of enantiomers (S-10_H and R-10_H; S-10_D and R-10_D) are resolved using Mosher analysis and the ratios are obtained using ¹H NMR spectroscopy.^70–71 All reactions were carried out using standard catalytic conditions at 60 °C. Figure here showcases the product generation using S-9_HD as an example. See SI for detailed analysis for both S-9_HD and R-9_HD.⁴¹