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. 2022 Aug 2;4(8):6103–6110. doi: 10.1021/acsapm.2c00914

Table 3. Yield of Insoluble Fraction and Thermal Characteristics of Polymers.

    DMTA
TGA
polymer yield of insoluble fraction [%]a Tg [°C]b Gr′ [MPa]c Tdec-10% [°C]d char yield [%]e
100D 97.0 ± 0.0 50 0.30 325 27
80D/20H 94.8 ± 0.9 30 0.09 327 25
60D/40H 97.7 ± 0.1 22 0.08 328 23
40D/60H 96.9 ± 0.4 43 0.24 328 21
20D/80H 95.0 ± 0.1 12 0.13 283 18
a

After 24 h of Soxhlet extraction with acetone.

b

Glass transition temperature determined by DMTA.

c

Storage shear modulus of cured resins in the rubbery plateau region.

d

Temperature at a weight loss of 10% obtained from TGA curves.

e

From TGA curves.