Table 2.
n-Hexadecane deconstructions with the 12 catalysts from the main library at 275, 325, and 375 °C
| Entry | Catalyst | Temp. (ºC) | Conv. (%) | C1-4 Yield (%)* | C5-16 Yield (%)* |
|---|---|---|---|---|---|
| 1 | SiO2-Al2O3 | 275 °C | 2.1 ± 0.2 | 0.0 | 2.1 |
| 2 | SiO2-Al2O3 | 325 °C | 3.8 ± 1.0 | 0.1 | 3.7 |
| 3 | SiO2-Al2O3 | 375 °C | 2.1 ± 0.2 | 0.1 | 2.0 |
| 4 | Zeo-Y_H | 275 °C | 4.5 ± 0.3 | 0.3 | 4.2 |
| 5 | Zeo-Y_H | 325 °C | 8.5 ± 0.5 | 0.7 | 7.7 |
| 6 | Zeo-Y_H | 375 °C | 26.7 ± 1.4 | 3.3 | 23.3 |
| 7 | ZSM-5_H | 275 °C | 13.7 ± 2.4 | 3.8 | 10.0 |
| 8 | ZSM-5_H | 325 °C | 91.6 ± 4.4 | 35.5 | 56.2 |
| 9 | ZSM-5_H | 375 °C | 98.0 ± 2.0 | 77.3 | 20.8 |
| 10 | Co/SiO2-Al2O3 | 275 °C | 2.3 ± 0.2 | 0.1 | 2.2 |
| 11 | Co/SiO2-Al2O3 | 325 °C | 2.3 ± 0.3 | 0.0 | 2.2 |
| 12 | Co/SiO2-Al2O3 | 375 °C | 2.4 ± 0.1 | 0.1 | 2.2 |
| 13 | Co/Zeo-Y_H | 275 °C | 1.9 ± 0.4 | 0.0 | 1.9 |
| 14 | Co/Zeo-Y_H | 325 °C | 5.5 ± 1.2 | 0.2 | 5.2 |
| 15 | Co/Zeo-Y_H | 375 °C | 6.1 ± 1.2 | 1.2 | 4.9 |
| 16 | Co/ZSM-5_H | 275 °C | 1.9 ± 0.1 | 0.1 | 1.8 |
| 17 | Co/ZSM-5_H | 325 °C | 5.9 ± 0.1 | 1.2 | 4.7 |
| 18 | Co/ZSM-5_H | 375 °C | 49.0 ± 3.7 | 12.7 | 36.3 |
| 19 | Ni/SiO2-Al2O3 | 275 °C | 2.6 ± 0.6 | 0.1 | 2.6 |
| 20 | Ni/SiO2-Al2O3 | 325 °C | 3.3 ± 1.4 | 0.1 | 3.2 |
| 21 | Ni/SiO2-Al2O3 | 375 °C | 3.8 ± 1.2 | 0.2 | 3.7 |
| 22 | Ni/Zeo-Y_H | 275 °C | 2.1 ± 0.6 | 0.6 | 1.5 |
| 23 | Ni/Zeo-Y_H | 325 °C | 4.4 ± 0.4 | 0.4 | 4.0 |
| 24 | Ni/Zeo-Y_H | 375 °C | 20.9 ± 1.3 | 0.4 | 20.5 |
| 25 | Ni/ZSM-5_H | 275 °C | 2.2 ± 0.2 | 0.3 | 1.9 |
| 26 | Ni/ZSM-5_H | 325 °C | 8.2 ± 1.8 | 0.5 | 7.7 |
| 27 | Ni/ZSM-5_H | 375 °C | 85.6 ± 4.1 | 28.2 | 57.3 |
| 28 | Ru/SiO2-Al2O3 | 275 °C | 95.6 ± 4.0 | 41.5 | 54.2 |
| 29 | Ru/SiO2-Al2O3 | 325 °C | 98.5 ± 0.3 | 75.8 | 22.6 |
| 30 | Ru/SiO2-Al2O3 | 375 °C | 99.8 ± 0.2 | 96.6 | 3.3 |
| 31 | Ru/Zeo-Y_H | 275 °C | 96.0 ± 0.9 | 56.6 | 39.3 |
| 32 | Ru/Zeo-Y_H | 325 °C | 99.6 ± 0.3 | 91.5 | 8.3 |
| 33 | Ru/Zeo-Y_H | 375 °C | 99.0 ± 1.0 | 92.4 | 6.9 |
| 34 | Ru/ZSM-5_H | 275 °C | 99.4 ± 0.6 | 92.8 | 6.6 |
| 35 | Ru/ZSM-5_H | 325 °C | 98.0 ± 2.0 | 99.7 | 0.3 |
| 36 | Ru/ZSM-5_H | 375 °C | 99.8 ± 0.2 | 98.8 | 1.1 |
Reaction conditions: n-hexadecane (1.59 g, 7.0 mmol), catalyst (0.1 g, metal loading = 2.5 wt%), S/C ratio (substrate/catalyst weight ratio) ~16, 45 bar H2, 2 h.
*All yields were calculated as the carbon yield and isomerized C16 (isoC16) are considered as products.