Table 1. GC-FID Operation Conditions.
| entry | parameters | values |
|---|---|---|
| 1 | injector temperature | 300 °C |
| 2 | injection volume | 1 μL |
| 3 | split ratio | 10 |
| 4 | column temperature program | |
| initial temperature | 50 °C hold 1 min | |
| rate 1 15 °C/min | 180 °C | |
| rate 2 7 °C/min | 230 °C | |
| rate 3 30 °C/min | 300 °C hold 10 min | |
| 5 | flow rate | 3 mL/min |
| 6 | FID temperature | 380 °C |
| 7 | carrier gas | nitrogen |