Table 3. Yield of Dimethyl Adipate under Optimized Conditions for Fly Ash Catalystsa.
entry | fly ash catalysts | % yield of dimethyl adipate |
---|---|---|
1 | FS-1 | 98 |
2 | FP-1 | 94 |
3 | FC-1 | 72 |
4 | without catalyst | 55 |
Reaction conditions: adipic acid: 1 mol, methanol: 6 mol, catalyst: 10% wt/wt, reaction time: 4 h, and reaction temperature: 200 °C.