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. 2022 Aug 5;10:951649. doi: 10.3389/fchem.2022.951649

TABLE 3.

Application of polymer monolithic columns in medicine.

Monolithic materials Initiator Matrix Type of column Analytical method LOD Recovery Ref
Allyl-β-CD-MMA/TAIC-EDMA AIBN crude extract of ephedra, lipopeptide antibiotics stainless steel column HPLC 1 ng/ml 100.27–103.77% 97.30–101.33% Zhao et al. (2021)
poly (DES-EGDMA) AIBN NSAIDs in spiked human plasma samples capillary column online in-tube SPME-HPLC 0.05–0.5 ng/ml 84.5–105.5% Wang et al. (2018a)
poly (ethylene glycol dimethacrylate-N-methacryloyl-(L)-phenylalanine methyl ester) (MIP S-CIT) AIBN enantioseparation of R,S-citalopram (R,S-CIT) in an aqueous solution capillary column CE + HPLC Derazshamshir et al. (2021)
DAIP-co-EDMA AIBN tussilagone in farfarae flos stainless-steel column SPE-HPLC 0.2 μg/ml 100.3–100.6% Wang L. et al. (2021)
AAPBA-co-DVB-co-MBAA AIBN benzimidazoles in animal capillary column in-tube SPME-MS 0.55–0.91 ng/g 72.5–92.4% Wu F. et al. (2021)
poly (GMA-SMX-co-EDMA) AIBN eight aromatic ketones and trypsin capillary column micro-HPLC Xiao et al. (2015)
AM-co-GMA-co-MBA-co-AMPS AIBN fifive alkaloids (piperine, nuciferine, kukoline, Berberine, tetrandrine) capillary column CEC 0.02–0.1 ug/ml 93.4–108.0% Chen et al. (2016)
poly (hexyl methacrylate) AIBN paracetamol and Chlorzoxazone capillary column nano-LC–UV 0.09–0.2 ug/ml 98.32–102.28% Salih et al. (2018)
(PHEA/TMPTA-EDMA) AIBN dioscin in human plasma stainless steel column SPE-HPLC-UV 96.61–113.73% Peng et al. (2020)
poly (GMA-EDMA) caffeic acid phenylamide, chlorogenic acid, piceatannol, nor-NOHA acetate capillary column HPLC Andre and Guillaume, (2021)
polymyxin-B AIBN 50 racemic pharmaceutical drugs capillary column nano-HPLC Ghanem et al. (2022)

3-Acrylamidophenylboronic acid (AAPBA); divinylbenzene (DVB); N, N′-Methylenebisacrylamide (MBAA); mass spectrometry (MS); ß-cyclodextrin (β-CD); methacrylate (MMA); ethylene dimethacrylate (EDMA); triallyl isocyanurate (TAIC); S-citalopram (S-CIT); R,S-citalopram (R,S-CIT); molecularly imprinted polymer (MIP); paracetamol (PAR); chlorzoxazone (CZN); liquid chromatography (LC); deep eutectic solvent (DES); ethylene glycol dimethacrylate (EGDMA); non-steroidal anti-inflflammatory drugs (NSAIDs); acrylamide (AM); glycidyl methacrylate (GMA); N,N′-methylenebisacrylamide (MBA); 2-acrylamido-2-methyl-1-propane-sulfonic acid (AMPS); capillary electrochromatography (CEC); sulfamethoxazole (SMX); diallyl isophthalate (DAIP); phenyl ether acrylate (PHEA); trimethylolpropane triacrylate (TMPTA).