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. Author manuscript; available in PMC: 2023 Feb 4.
Published in final edited form as: ACS Catal. 2022 Jan 20;12(3):1905–1918. doi: 10.1021/acscatal.1c05586

Scheme 4. Synthesis of (FI)Co(Cl)(DMA)a.

Scheme 4.

aSee SI for details; bRepresentation of the molecular structure of (2,6-di-i-PrPhdi-t-BuFI)CoCl(DMA) at 30% probability ellipsoids; hydrogen atoms omitted for clarity. Selected bond distances (Å) and angles (°): Co1–O1 1.9025(12), Co1–O2 1.9882(13), Co1–N1 1.9864(14), Co1–Cl1 2.2258(5); O1–Co1–N1 96.12(5), Cl1–Co1–O2 118.34(4).