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. Author manuscript; available in PMC: 2023 Feb 4.
Published in final edited form as: ACS Catal. 2022 Jan 20;12(3):1905–1918. doi: 10.1021/acscatal.1c05586

Scheme 5. Preparation of [(FI)CoCl(DMA)]2.

Scheme 5.

aInseparable from bisligand chelate (4-F-PhFI)2Co (15c). Sample represents an 80:20 molar ratio of 11c:15c; yield is with respect to desired compound.