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Optimization of ligand structurea
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Reactions performed on 0.10-mmol scale using 5 mol% CoCl2 and 5 mol% ligand; yields determined by GC-FID using n-dodecane as an internal standard. Mass balances >100% reflect error of GC yields. DMA = N,N-dimethylacetamide; neo = neo-pentylglycol.
