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. 2022 Jul 8;40(7):634–643. [Article in Chinese] doi: 10.3724/SP.J.1123.2022.01011

表 2.

不同洗脱条件下唑虫酯及其氧化产物异构体的分离度

Elution condition number φ(Mobile phase B)/% Acquisition time/min Rs1 Rs2 Rs3 Rs4
1 20-95-95-20 5-35-40-45 0.53 1.37 0.96 2.93
2 40-95-95-40-40 5-50-65-70-80 1.03 2.05 1.31 3.88
3 40-70-95-95-40-40 5-35-40-45-48-50 1.12 2.10 1.34 3.97
4 42-55-95-95-42-42 4-55-58-62-65-70 1.62 2.64 1.62 5.47
5 42-48-42-42 2.5-66-67-70 1.63 2.81 1.78 6.03
6 43-46-43-43 2.5-57-58-60 1.63 2.83 1.74 5.82

Mobile phase B: acetonitrile; Rs1: resolution of peaks 1 and 2 in Fig. 3; Rs2: resolution of peaks 2 and 3 in Fig. 3; Rs3: resolution of peaks 3 and 4 in Fig. 3; Rs4: resolution of peaks 5 and 6 in Fig. 3.