表 3.
唑虫酯及其氧化产物异构体的线性关系和基质效应
| Analyte | Matrix | Linear range/(μg/L) | Standard curve | R2 | Matrix effect/% |
|---|---|---|---|---|---|
| RS-Pyr | acetonitrile | 0.25-500 | Y=8.7×107X-1.6×104 | 0.9999 | |
| water spinach | 1.25-1250 | Y=1.1×108X+4.3×105 | 0.9998 | 26.8 | |
| pakchoi | 1.25-1250 | Y=9.3×107X+1.3×105 | 0.9999 | 6.1 | |
| SS-Pyr | acetonitrile | 0.25-500 | Y=1.1×108X-2.6×103 | 0.9999 | |
| water spinach | 1.25-1250 | Y=1.1×108X+5.1×105 | 0.9998 | 1.9 | |
| pakchoi | 1.25-1250 | Y=1.2×108X+1.6×106 | 0.9987 | 10.2 | |
| RR-Pyr | acetonitrile | 0.25-500 | Y=1.1×108X+3.4×104 | 0.9999 | |
| water spinach | 1.25-1250 | Y=1.1×108X+5.0×105 | 0.9998 | 0.7 | |
| pakchoi | 1.25-1250 | Y=1.2×108X+1.6×106 | 0.9987 | 9.0 | |
| SR-Pyr | acetonitrile | 0.25-500 | Y=9.2×107X+1.4×104 | 0.9999 | |
| water spinach | 1.25-1250 | Y=1.1×108X+4.4×105 | 0.9998 | 20.7 | |
| pakchoi | 1.25-1250 | Y=1.2×108X+1.4×106 | 0.9988 | 30.6 | |
| S-(Pyr+O) | acetonitrile | 0.5-100 | Y=6.5×107X+2.1×104 | 0.9999 | |
| water spinach | 2.5-2500 | Y=6.9×107X+8.3×105 | 0.9996 | 7.3 | |
| pakchoi | 2.5-2500 | Y=7.6×107X+2.2×106 | 0.9981 | 17.1 | |
| R-(Pyr+O) | acetonitrile | 0.5-100 | Y=6.6×107X+2.7×104 | 0.9999 | |
| water spinach | 2.5-2500 | Y=7.2×107X+6.9×105 | 0.9997 | 9.0 | |
| pakchoi | 2.5-2500 | Y=7.8×107X+2.0×106 | 0.9999 | 18.2 |
Y: peak area; X: mass concentration, μg/L; R2: correlation coefficient.