表3.
7种苯氧羧酸类除草剂的回收率和精密度(n=5)
| Analyte | Spiked/ (μg/L) |
Recovery/ % |
RSDs/% | Analyte | Spiked/ (μg/L) |
Recovery/ % |
RSDs/% | ||
|---|---|---|---|---|---|---|---|---|---|
| Intra-day | Inter-day | Intra-day | Inter-day | ||||||
| 4-CPA | 0.005 | 80 | 5.7 | 4.2 | 2,4,5-T | 0.005 | 88 | 4.7 | 6.0 |
| 0.05 | 89 | 2.4 | 7.3 | 0.05 | 92 | 2.9 | 10.7 | ||
| 0.2 | 92 | 1.4 | 5.6 | 0.2 | 89 | 4.7 | 6.0 | ||
| PB | 0.005 | 81 | 8.8 | 7.2 | 2,4-DB` | 0.005 | 81 | 8.9 | 12.3 |
| 0.05 | 93 | 4.4 | 6.0 | 0.05 | 85 | 7.9 | 12.6 | ||
| 0.2 | 91 | 3.9 | 4.9 | 0.2 | 82 | 8.0 | 9.8 | ||
| 2,4-D | 0.005 | 81 | 7.4 | 9.8 | 2,4,5-TP | 0.005 | 102 | 9.4 | 10.8 |
| 0.05 | 91 | 3.9 | 5.2 | 0.05 | 91 | 3.2 | 8.2 | ||
| 0.2 | 89 | 3.1 | 4.6 | 0.2 | 88 | 3.1 | 8.2 | ||
| MCPA | 0.005 | 91 | 7.0 | 5.2 | |||||
| 0.05 | 92 | 3.0 | 7.3 | ||||||
| 0.2 | 84 | 2.8 | 5.1 | ||||||