表2.
本方法与文献报道的水产品中丁香酚类麻醉剂检测方法比较
Method | Samples | Linear range/ (μg/L) |
LODs/(μg/kg) | Ref. | |||
---|---|---|---|---|---|---|---|
Eugenol | Eugenyl acetate | Methyl eugenol | |||||
SPE-GC-MS | fish | 5- | 500 | 0.4 | - | 0.2 | [4] |
DSPE-HPLC-MS | shrimp, crab, carp | 5- | 500 | 1.47 | - | - | [8] |
LLE-HPLC-UV | tilapia | 100- | 10000 | 30 | - | - | [9] |
MISPE-HPLC-UV | grouper, prawn | 50- | 10000 | 15 | - | 15 | [10] |
F-COP-SPME-HPLC-UV | tilapia, shrimp | 10- | 1000 | 2.9 | 4.5 | 3.3 | this work |
DSPE: dispersive SPE; LLE: liquid-liquid extration; MISPE: molecularly imprinted solid phase extraction. -: not detected.