Table 7. Recyclability of the ChsB–Pd 3 Catalysta.
| number of cycle | yield (%) | TON | TOF (h–1) |
|---|---|---|---|
| 1st | 94 | 18431 | 110,586 |
| 2nd | 94 | 18431 | 110,586 |
| 3rd | 92 | 18039 | 108,234 |
| 4th | 92 | 18039 | 108,234 |
| 5th | 90 | 17647 | 105,882 |
Reaction conditions: 4-bromoanisole 4 (1 mmol), phenylboronic acid 5a (1.2 mmol), Pd catalyst (5.1 × 10–3 mol %), and NaHCO3 (2 mmol) in EtOH/H2O (1:1, 3 ml), 80 °C for 10 min under the MW condition with Pmax = 200 W. Isolated yield.