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. 2022 Aug 10;7(33):28831–28848. doi: 10.1021/acsomega.2c01809

Table 7. Recyclability of the ChsB–Pd 3 Catalysta.

number of cycle yield (%) TON TOF (h–1)
1st 94 18431 110,586
2nd 94 18431 110,586
3rd 92 18039 108,234
4th 92 18039 108,234
5th 90 17647 105,882
a

Reaction conditions: 4-bromoanisole 4 (1 mmol), phenylboronic acid 5a (1.2 mmol), Pd catalyst (5.1 × 10–3 mol %), and NaHCO3 (2 mmol) in EtOH/H2O (1:1, 3 ml), 80 °C for 10 min under the MW condition with Pmax = 200 W. Isolated yield.