| CCDC |
2173544 |
| chemical formula |
C34H26F8N2O2
|
|
Mr
|
646.57 |
| crystal system, space group |
triclinic, P1̅ |
| temperature
(K) |
150 (2) |
|
a, b, c (Å) |
9.9381 (6), 11.7975
(7),
14.0204 (9) |
| α, β, γ (deg) |
106.603 (5), 105.040 (6),
99.032 (5) |
|
V (Å3) |
1473.11 (17) |
| Z |
2 |
| density (calculated)g/cm–3
|
1.458 |
|
F(000) |
664 |
| radiation type |
Cu Kα |
| wavelength (λ) |
1.54184 |
| μ (mm–1) |
1.088 |
| crystal size (mm) |
0.28 × 0.24 × 0.17 |
| data collection |
|
| diffractometer |
Bruker APEXII CCD |
| absorption correction |
multiscan (SADABS; Bruker,
2007) |
| no.
of measured, independent,
and observed [I > 2σ(I)] reflections |
9288, 4663, 3772 |
|
Rint
|
0.034 |
| θ range for data collection (deg) |
3.474–62.769 |
| index
ranges |
–11 ≤ h ≤ 11, –13 ≤ k ≤ 12, –15 ≤ l ≤ 16 |
| data
refinement |
|
|
R[F2 > 2σ(F2)], wR(F2), S
|
0.042, 0.116, 1.04 |
| no. of reflections |
4663 |
| no. of parameters |
426 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å–3) |
0.32, −0.27 |
