Fig. 4. (a–d) Time dependent flow properties of the solvent-free PS-OS@SiNR-11 composite at 35 °C. Tiny air bubbles trapped in the viscous liquid can also be seen. The images were taken with the spatula containing the sample suspended in air, and the liquid drop pointing towards the ground. (e) Differential scanning calorimetry shows the glass transition temperature (@ −55 °C for all PS-OS@SiNR samples), crystallization temperature (Tc), and melting transition temperatures (Tm) for all the samples.
