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. 2022 Aug 31;12(38):24590–24595. doi: 10.1039/d2ra02762c

The 13C NMR data for 1–7.

Position 1a 2a 3b 4a 5a 6a 7a
δ C δ C δ C δ C δ C δ C δ C
1 39.4, CH2 43.3, CH2 43.1, CH2 35.8, CH2 79.9, CH 39.6, CH2 43.8, CH2
2 27.8, CH2 28.0, CH2 28.4, CH2 27.0, CH2 35.8, CH2 28.0, CH2 28.2, CH2
3 54.2, CH 53.9, CH 53.5, CH 52.1, CH 49.0, CH 54.0, CH 54.0, CH
4 55.2, CH 51.5, CH 56.1, CH 44.3, CH 55.8, CH 49.1, CH 53.1, CH
5 48.8, C 43.4, C 42.3, C 56.3, C 45.4, C 47.5, C 43.9, C
6 81.5, CH 52.5, CH2 58.1, CH2 208.0, C 40.8, CH2 87.3, CH 51.5, CH2
7 131.7, CH 70.6, CH 218.6, C 127.1, C 123.5, CH 204.3, C 74.1, CH
8 136.6, C 141.4, C 48.4, CH 152.2, C 140.6, C 134.9, C 155.0, C
9 36.9, CH2 126.3, CH 27.1, CH2 35.5, CH2 37.0, CH2 143.4, CH 34.0, CH2
10 24.1, CH2 27.8, CH2 18.9, CH3 22.8, CH2 24.3, CH2 29.9, CH2 27.7, CH2
11 27.1, CH3 23.5, CH3 74.1, C 28.3, CH3 27.4, CH3 21.9, CH3 113.1, CH2
12 75.0, C 74.8, C 21.2, CH3 73.9, C 74.8, C 74.3, C 74.6, C
13 14.4, CH3 18.9, CH3 11.1, CH3 20.1, CH3 13.5, CH3 14.0, CH3 19.7, CH3
14 32.3, CH3 32.4, CH3 32.1, CH3 32.5, CH3 32.1, CH3 32.9, CH3 32.0, CH3
15 26.8, CH3 27.2, CH3 27.3, CH3 27.2, CH3 27.1, CH3 27.1, CH3 27.7, CH3
a

13C (150 MHz) NMR data in CD3OD.

b

13C (150 MHz) NMR data in CDCl3.