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. 2022 May 13;78(Pt 6):563–567. doi: 10.1107/S2056989022004789
O1—C10 1.2177 (15) O4—C22 1.2207 (16)
O2—C10 1.3165 (15) O5—C22 1.3180 (16)
O2—H2A 0.843 (9) O5—H5A 0.860 (9)
O3—C11 1.2221 (16) O6—C23 1.2234 (17)
C1—C6 1.3950 (19) C13—C18 1.396 (2)
C1—C2 1.3961 (18) C13—C14 1.3981 (19)
C1—C7 1.4704 (18) C13—C19 1.4722 (19)
C2—C3 1.3885 (19) C14—C15 1.387 (2)
C2—H2 0.9500 C14—H14 0.9500
C3—C4 1.381 (2) C15—C16 1.379 (2)
C3—H3 0.9500 C15—H15 0.9500
C4—C5 1.384 (2) C16—C17 1.387 (2)
C4—H4 0.9500 C16—H16 0.9500
C5—C6 1.386 (2) C17—C18 1.385 (2)
C5—H5 0.9500 C17—H17 0.9500
C6—H6 0.9500 C18—H18 0.9500
C7—C8 1.3458 (18) C19—C20 1.3479 (18)
C7—H7 0.9500 C19—H19 0.9500
C8—C11 1.4885 (18) C20—C23 1.4887 (19)
C8—C9 1.5046 (17) C20—C21 1.5011 (18)
C9—C10 1.5002 (17) C21—C22 1.4949 (18)
C9—H9A 0.9900 C21—H21A 0.9900
C9—H9B 0.9900 C21—H21B 0.9900
C11—C12 1.5040 (18) C23—C24 1.497 (2)
C12—H12A 0.9800 C24—H24A 0.9800
C12—H12B 0.9800 C24—H24B 0.9800
C12—H12C 0.9800 C24—H24C 0.9800
C10—O2—H2A 109.3 (13) C22—O5—H5A 109.9 (14)
C6—C1—C2 118.28 (12) C18—C13—C14 118.30 (13)
C6—C1—C7 124.71 (12) C18—C13—C19 123.78 (12)
C2—C1—C7 117.00 (11) C14—C13—C19 117.92 (12)
C3—C2—C1 120.89 (13) C15—C14—C13 120.54 (14)
C3—C2—H2 119.6 C15—C14—H14 119.7
C1—C2—H2 119.6 C13—C14—H14 119.7
C4—C3—C2 119.83 (13) C16—C15—C14 120.35 (14)
C4—C3—H3 120.1 C16—C15—H15 119.8
C2—C3—H3 120.1 C14—C15—H15 119.8
C3—C4—C5 120.05 (13) C15—C16—C17 119.83 (14)
C3—C4—H4 120.0 C15—C16—H16 120.1
C5—C4—H4 120.0 C17—C16—H16 120.1
C4—C5—C6 120.11 (14) C18—C17—C16 120.04 (14)
C4—C5—H5 119.9 C18—C17—H17 120.0
C6—C5—H5 119.9 C16—C17—H17 120.0
C5—C6—C1 120.69 (13) C17—C18—C13 120.83 (13)
C5—C6—H6 119.7 C17—C18—H18 119.6
C1—C6—H6 119.7 C13—C18—H18 119.6
C8—C7—C1 128.26 (12) C20—C19—C13 127.13 (13)
C8—C7—H7 115.9 C20—C19—H19 116.4
C1—C7—H7 115.9 C13—C19—H19 116.4
C7—C8—C11 120.96 (12) C19—C20—C23 121.25 (12)
C7—C8—C9 124.70 (12) C19—C20—C21 124.47 (12)
C11—C8—C9 114.30 (11) C23—C20—C21 114.03 (11)
C10—C9—C8 112.85 (10) C22—C21—C20 114.69 (11)
C10—C9—H9A 109.0 C22—C21—H21A 108.6
C8—C9—H9A 109.0 C20—C21—H21A 108.6
C10—C9—H9B 109.0 C22—C21—H21B 108.6
C8—C9—H9B 109.0 C20—C21—H21B 108.6
H9A—C9—H9B 107.8 H21A—C21—H21B 107.6
O1—C10—O2 123.54 (11) O4—C22—O5 123.84 (12)
O1—C10—C9 123.69 (11) O4—C22—C21 124.00 (12)
O2—C10—C9 112.77 (11) O5—C22—C21 112.16 (11)
O3—C11—C8 119.59 (12) O6—C23—C20 119.67 (13)
O3—C11—C12 120.27 (12) O6—C23—C24 120.19 (13)
C8—C11—C12 120.14 (11) C20—C23—C24 120.14 (12)
C11—C12—H12A 109.5 C23—C24—H24A 109.5
C11—C12—H12B 109.5 C23—C24—H24B 109.5
H12A—C12—H12B 109.5 H24A—C24—H24B 109.5
C11—C12—H12C 109.5 C23—C24—H24C 109.5
H12A—C12—H12C 109.5 H24A—C24—H24C 109.5
H12B—C12—H12C 109.5 H24B—C24—H24C 109.5
C6—C1—C2—C3 −4.16 (19) C18—C13—C14—C15 3.5 (2)
C7—C1—C2—C3 174.86 (12) C19—C13—C14—C15 −176.45 (14)
C1—C2—C3—C4 1.8 (2) C13—C14—C15—C16 −0.9 (2)
C2—C3—C4—C5 1.4 (2) C14—C15—C16—C17 −1.6 (3)
C3—C4—C5—C6 −2.2 (2) C15—C16—C17—C18 1.5 (2)
C4—C5—C6—C1 −0.3 (2) C16—C17—C18—C13 1.2 (2)
C2—C1—C6—C5 3.4 (2) C14—C13—C18—C17 −3.6 (2)
C7—C1—C6—C5 −175.55 (13) C19—C13—C18—C17 176.32 (14)
C6—C1—C7—C8 35.8 (2) C18—C13—C19—C20 −40.4 (2)
C2—C1—C7—C8 −143.15 (14) C14—C13—C19—C20 139.55 (15)
C1—C7—C8—C11 176.80 (12) C13—C19—C20—C23 −176.30 (12)
C1—C7—C8—C9 −0.8 (2) C13—C19—C20—C21 −2.2 (2)
C7—C8—C9—C10 −98.93 (15) C19—C20—C21—C22 109.04 (15)
C11—C8—C9—C10 83.34 (14) C23—C20—C21—C22 −76.51 (14)
C8—C9—C10—O1 −1.06 (18) C20—C21—C22—O4 −3.04 (19)
C8—C9—C10—O2 179.02 (11) C20—C21—C22—O5 176.86 (11)
C7—C8—C11—O3 178.72 (13) C19—C20—C23—O6 171.99 (13)
C9—C8—C11—O3 −3.45 (18) C21—C20—C23—O6 −2.65 (18)
C7—C8—C11—C12 −1.81 (19) C19—C20—C23—C24 −8.0 (2)
C9—C8—C11—C12 176.02 (12) C21—C20—C23—C24 177.38 (12)